Cleanroom

From Concept to Wafer: One-Stop Semiconductor Technologies

© Eric Shambroom Photography 2020
© Eric Shambroom Photography 2020

The cleanrooms at Fraunhofer ISIT combine research, technology development, and manufacturing into a seamless process chain. Cleanroom infrastructures designed for 200-mm technologies enable both established semiconductor processes and the integration of sophisticated materials and post-CMOS technologies.

 

ISIT’s particular strength lies in the interplay of process development, manufacturing, integration, assembly and interconnection technology, and characterization—all of which are seamlessly integrated at a single location. This enables us to develop new processes, implement complex process sequences, and support the development of innovative components for microsystems technology and power electronics from the initial concept through to a fully functional device*.

 

 

 

 

 

 

 

 

 

 

 

* ISIT’s facilities have been ISO 9001-certified for many years.

Discover our technologies and learn how we turn challenging ideas into reliable processes and innovative components.

Optimally Coordinating Material, Coating, and Process

Both thin and thick functional layers must reliably fulfill their (di-)electric, mechanical, optical, or piezoelectric functions while also being compatible with the entire manufacturing process. Key factors here include the material system, the required layer thickness, the available temperature budget, conformality on a wide variety of structured surfaces, and the properties of the substrate. Subsequent manufacturing steps, such as lithography, etching, bonding, or packaging, must also be taken into account early on. The goal is to reproducibly produce insulating, conductive, semiconducting, and functional layers for use in MEMS and power electronic components and to integrate their deposition into coordinated process chains. An inappropriate choice of process or uncoordinated process parameters can lead to loss of function, insufficient layer quality, or limited patterning capability of the device.

What We Offer

  • CVD: LPCVD and PECVD for silicon compounds and dielectric or semiconducting layers.
  • PVD: Sputtering and electron beam evaporation for metals, metal compounds, and magnetic and piezoelectric functional layers.
  • ALD: thermal, plasma-assisted, and ozone-based processes.
  • EpiPoly technology for p- or n-doped silicon and thick polysilicon layers up to a thickness of 100 µm.
  • Electroplating for Cu, Ni, Au, and Sn layers.
  • Polymer coating with parylene.
  • Project-specific needs analysis, customized selection of suitable processes and process windows, and their integration with lithography, patterning, and metrology.

Equipment & Technology

Procedure

Material Portfolio

Selected Equipment

LPCVD

SiN, dry SiO, wet SiO, HTO, TEOS, a-Si, poly-Si; doped and undoped variants

ASM 400; ASM A400 DUO

PECVD

SiO (silane- and TEOS-based), SiN, SiON, and a-Si; depending on the layer system and doping

Applied Materials Centura PECVD

PVD / Sputtering

Ti, Cu, Cr, WTi, Au, TiN, TiO, Pt, AlCu, AlN, AlScN, Mo, FeCoB

Evatec LLS EVO2;

Evatec Clusterline 200

E-Beam-Evaporation

Ti, Ta, Al, Ni, Ag, Pt, Au, Ir, Ge

Evatec BAK760;

Evatec BAK761

ALD

SiN, SiO, TiN, TiO, AlO, HfO; thermal, plasma-assisted, ozone-based

Picosun R-200;

Picosun Sunale R-series

EpiPoly

p- or n-doped silicon; thick polysilicon

ASM Epsilon 2000;

ASM400 Duo

Galvanik

Cu, Ni, Au, Sn

Semsysco Triton

Polymer Coating

Parylene

PPS Parylene Coater

Use Cases

  • Dielectric and passivation layers
  • Metallization and electrical contacts
  • Piezoelectric, ferroelectric, and magnetic functional layers
  • Getter and protective layers
  • Epitaxial and thick polysilicon layers
  • Electrolytic structures and bond frames

Advantages

  • A broad and coordinated portfolio of gas-phase, physical, single-atom-layer, epitaxial, electrochemical, and polymer-based processes.
  • Combination of deposition, patterning, and characterization within a single technological infrastructure.
  • Development and refinement of individual process modules, as well as their integration into application-specific end-to-end manufacturing flows

Designing Lithography Processes to Be Precise and Reproducible

Lithography precisely reproduces mask patterns in photoresist on wafer surfaces, with or without existing topography, and lays the foundation for subsequent etching, deposition, electroplating, or lift-off processes. Key challenges include controlling and maintaining the critical feature width across the entire wafer, achieving high reproducibility from wafer to wafer, and ensuring highly accurate alignment of different lithography layers. At the same time, both thin and thick resist layers must be applied uniformly and completely cover a wide variety of topographies. Substrates made of specialty materials such as glass, GaN, or SiC also place special demands on coating, alignment, and exposure. The goal is consistently stable, reproducible, and integrable pattern transfer. Deviations in CD, overlay, or resist thickness can distort geometries, shift functional layers, and thereby impair overall functionality, process yield, and transferability.

What We Offer

  • Optical i-line stepper lithography with 1:2 and 1:5 projection.
  • Contact and proximity exposure with a mask aligner, including front- and back-side alignment.
  • Spin and spray coating; positive and negative resists; thin and thick resists.
  • Multilayer lithography, lift-off, high-resolution, and thick resist processes.
  • Additional services: process and recipe development, resist selection, dose/focus optimization, process integration, CD/overlay characterization, profilometry, prototyping, and technology transfer.

Equipment & Technology

Process step

Equipment

Features

Coating / Developing

SVG 90;

SÜSS ACS200

Automated spin coating; ACS200 additionally equipped with spray coating as well as bake, cool, and development modules

Stepper

Canon FPA-3000iW;

Canon FPA-3030i5+

i-line; 1:2 (CD: ~800 nm) and 1:5 (CD: ~300 nm) projection;

FPA-3030i5+ with IR and back-side alignment

Mask Aligner

SÜSS MA200 Compact

Contact/Proximity;

Front- and back-side alignment (CD: 1 µm)

Metrology

Hitachi 9260 CDSEM;

KLA Archer XT+

CD and overlay metrology for 200-mm wafers

Bake

Hotplates;

Heraeus Oven; Despatch Oven

Ovens up to 230°C and 300°C, respectively, according to the supplementary document

Use Cases

  • Optimized thin-film resist processing for submicrometer feature widths at the resolution limits of existing stepper exposure systems.
  • Thick-film or multilayer resist processing for the fabrication of electroplated structures up to 80 µm in height and with high aspect ratios.
  • Lithography on high topographies using spray or multiple spin coating.

Advantages

  • A tailored suite of services encompassing coating, exposure, development, and metrology.
  • Integration with on-site deposition, etching, and lift-off processes.
  • A broad portfolio of resists and substrates for MEMS, III-V, post-CMOS, and packaging applications.
  • Individual processes, process development, and integrated process chains—all from a single source. A coordinated portfolio of coating, exposure, development, and metrology services.
  • Integration with on-site deposition, etching, and lift-off processes.
  • A broad portfolio of resists and substrates for MEMS, III-V, post-CMOS, and packaging applications.
  • Individual processes, process development, and integrated process chains—all from a single source.

Precisely Structure Layers and Protect Surfaces

In layer and wafer patterning, different materials must be selectively removed without adversely affecting the mask, adjacent layers, or the substrate. Material stacks consisting of dielectrics, metals, functional layers, (poly)silicon, and thin or thick dielectrics each require tailored dry or wet etching processes. Depending on the component, isotropic or anisotropic etch profiles, high aspect ratios, and very small or very large apertures in a wide variety of materials are required. At the same time, cleaning, resist removal, and thermal post-treatment must be compatible with the temperature budget of the process chain. The goal is to achieve reproducible geometry with appropriate selectivity and good surface quality relative to the underlying interface. Inappropriate processes can cause profile deviations, material damage, residues, or loss of functionality.

What We Offer

  • Dry etching: Etching of dielectric layers, metals, and hard materials, as well as deep etching of silicon (DRIE); also processes for functional layers, glass, and thick oxide layers.
  • Wet etching for a broad range of materials, as well as spin-etch processes for selected metals.
  • Cleaning: RCA cleaning with SC-1 and SC-2, Piranha cleaning, diluted HF, and DSP and HVS processes.
  • Chemical resist stripping and lift-off.
  • Thermal processes: Annealing and Rapid Thermal Processing (RTP).
  • Project-specific needs analysis, selection of suitable patterning methods and process windows, and their integration with lithography and metrology. Upstream and downstream coating and patterning steps are taken into account holistically.

Equipment & Technology

Process family

Materials / Task

Selected Equipment

Dielectric Etch

Si, SiN, SiO, SiON and other silicon compounds

Applied Materials P5000

Plasma-based metal etching

Al, AlCu, Ti, TiN, Ta, Mo;

 

Applied Materials Centura Metal Etch

Ion beam etching

Ti, Pt, WTi, Cu, FeCoB, AlN, AlScN

Scia Mill 200

GaN Etch

GaN, AlGaN

Applied Materials Centura Metal Etch, KLA fxP

Hard Material Etch

Ta, Pt, SiO, AlScN

STS APS

Silicon DRIE

Deep silicon etching and Bosch processes

SPTS Pegasus;

Lam TCP 9400

Piezoelectric Layers

AlN, AlScN

Applied Materials Centura Metal Etch;

KLA fxP Synapse

Silicon / Glass / Thick Oxides

(D)RIE of Si; glass and thick oxide layers

KLA c2L Rapier;

KLA c2L Synapse

Gas-phase etching

Selective etching of SiO (sacrificial layers, exposure processes)

KLA Primaxx

Wet chemical etching

Si, SiN, SiO, SiON, Al(Sc)N, Glas

Cu, Al, AlCu, WTi, Mo, Ti, TiN, Cr, Au, Ge

Ramgraber tank;

AP&S spin etcher

Annealing

200–1150 °C; 30 Pa to atmospheric pressure

ASM400;

Koyo VF-1000LP

RTP

400–1100 °C

Mattson 2800

Use Cases

  • Deep silicon etching and Bosch processes for the fabrication of MEMS structures.
  • Pattern formation of metallic contact and electrode layers.
  • Pattern formation of AlN/AlScN and other functional layers.
  • Processing of glass and thick oxide layers.
  • Cleaning and stripping processes within integrated process chains.

Advantages

  • Specialized plasma systems for various material classes and structural profiles.
  • Combination of dry etching, wet chemical etching, cleaning, thermal processes, and metrology.
  • Support for individual etching modules as well as complete structure transfer chains.

Creating Stable Connections for Reliable Wafer Packages

Wafer bonding and (vacuum) wafer-level packaging (vWLP) enable the bonding of flat, patterned, or specially shaped wafers and protect sensitive structures through functional or hermetic encapsulation. The quality of the bond depends on material pairing, surface condition, bond frame, temperature budget, alignment, and the desired internal atmosphere. At the same time, upstream and downstream steps such as cleaning, metallization, lithography, etching, wafer thinning, and characterization must be taken into account. The goal is a mechanically stable, sufficiently tight, and electrically functional bond that withstands subsequent operational and reliability requirements. Unsuitable surfaces or process conditions can lead to incomplete bond areas, leaks, warping, contact problems, or premature failure.

What We Offer

  • Anodic, eutectic, glass frit, and direct/fusion wafer bonding.
  • Temporary, resist-based bonding using carrier concepts.
  • Wafer-level packaging with application-specific process combinations.
  • Glass and silicon cap connections with a defined internal atmosphere and application-specific capping.

Equipment & Technology

Processes

Materials / Integration

Equipment

Glass Frit Bonding

Encapsulation with Glass Frit Bonding Frames

SÜSS SB8e

Anodic Bonding

Silicon and Glass Systems

SÜSS SB8e

Metal Bonding / Eutectic Bonding

AuSi- and AlGe-based bonding

SÜSS SB8e

Fusion Bonding

Direct wafer bonding; material- and surface-dependent

SÜSS SB8e

Temporary Bonding

Resist-based temporary carrier concepts

EVG bonding/debonding system; application-specific in-house developments

Use Cases

  • Encapsulation using glass or silicon cap wafers.
  • Wafer-level packaging with a controlled internal atmosphere.
  • AuSi- and AlGe-based eutectic compounds.
  • Temporary carrier concepts for subsequent wafer processing.

Advantages

  • Bonding and vWLP can be combined with upstream and downstream cleanroom and characterization processes.
  • Application-specific selection from among several wafer bonding methods.
  • Support ranging from individual processes to integrated process chains.

Precise wafer processing for defined surfaces and geometries

Mechanical wafer processing and chemical-mechanical polishing (CMP) adjust a wafer’s thickness, surface, and geometry to meet the requirements of subsequent processing or characterization steps. During grinding, material must be removed efficiently without causing excessive damage, warping, or breakage. CMP planarization at ISIT enables highly controlled material removal and the planarization of qualified material systems. This process takes into account the different materials as well as contamination classes. During separation via bladedicing, the cutting path, alignment, and mechanical stress must be tailored to the device and substrate. The goals are defined final thicknesses, flat and suitable surfaces, and precisely separated components. Inappropriate processing parameters can cause chipping, cracks, surface damage, dimensional deviations, or reduced component yield.

What We Offer

  • Grinding for thickness reduction of silicon and glass.
  • Semi-automatic and fully automatic blade dicing.
  • IR alignment, ultrasonic-assisted dicing, and circular cutting.
  • CMP in a CMOS-compatible process line, as well as material tracks for Si, SiO, SiC, and GaN.

Equipment & Technology

Technology

Capability

Equipment / Special Features

Grinding

Thickness reduction of silicon and glass;

AlN- and SiC-based substrates

Disco DFG 8540;

Disco DAG 810

Dicing

Semi-automatic and fully automatic blade dicing

Disco DAD3350, DFD6340, 6240; IR alignment, ultrasonic assistance, circular cutting

CMP – CMOS FEOL

CMOS-compatible planarization

Ebara FREX200

CMP – Material track

Si, SiO, GaN; metal-contaminated line

Ebara FREX200

CMP – expanded portfolio

Si, SiO, SiC, GaN; metal-contaminated line

Ebara FREX200

Use Cases

  • Substrate thickness adjustment before, during, and after wafer processing or packaging.
  • Planarization of Si, SiO, SiC, or GaN surfaces.
  • Separation of wafers and devices using IR alignment.
  • Circular cutting or ultrasonic-assisted dicing for special geometries or materials.

Advantages

  • Grinding and CMP as complementary process modules.
  • Support for various materials and contamination classes.
  • On-site integration of wafer processing, debonding, packaging, and characterization.

Measuring, Evaluating, and Effectively Securing Processes

Metrology, characterization, and reliability testing provide the data foundation for process control and component evaluation. Depending on the specific application, it may be necessary to determine layer thickness, geometry, surface structure, material properties, electrical characteristics, or behavior under thermal, mechanical, electrical, and environmental stresses. The challenge lies in combining appropriate methods for wafers, chips, and packages and assigning measurement results to the respective process steps. The goal is to achieve a traceable and robust evaluation throughout the entire development chain so that deviations can be detected early and process windows can be validated. Inappropriate or incomplete characterization can leave relevant failure mechanisms undetected and limit the comparability and validity of development and reliability results.

What We Offer

  • Material and Structural Metrology in the Cleanroom: Reflectometry, ResMap, optical inspection, wafer geometry, white-light interferometry, profilometry, CD-SEM, and particle scanning.
  • Analytical Laboratory: AFM, XRD, XRR, SEM, X-ray analysis, XRF, laser microscopy, and 2D/3D X-ray tomography, double-beam laser interferometer (DBLI).
  • Electrical characterization using semi-automatic and fully automatic wafer or chip testers.
  • Reliability and environmental testing, as well as combined electrical-thermal-mechanical tests.

Equipment & Technology

Field

Method / key data

Note

Cleanroom Metrology

Reflectometry, ResMap, optical inspection, wafer geometry, white-light interferometry, profilometry, CD-SEM, particle scan

In-process

Analytical Laboratory

AFM, XRD, XRR, SEM, X-ray analysis, XRF, laser microscopy, 2D/3D X-ray tomography, double-beam laser interferometer (DBLI)

Material and Structural Analysis

Electrical Laboratories

Resistance, capacitance, frequency, and phase angle measurements

Wafer or chip probers, depending on the application

Reliability

Electrical, thermal, and mechanical tests; −70 to 180 °C; 10 to 98% relative humidity; thermal stress up to 1300 °C

Automated and combined tests

Use Cases

  • In-process CD, overlay, profile, and layer inspection.
  • Material analysis and structural characterization.
  • Electrical wafer and chip characterization.
  • Environmental and reliability assessment of components and packages.

Advantages

  • Integration of cleanroom metrology, laboratory analysis, electrical characterization, and reliability testing.
  • Evaluation across the entire development chain rather than isolated individual measurements.
  • Automated and combined testing for components and packages.

 

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